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TM4000Plus_frontal perspective

TM4000 Series Tabletop SEM

Beyond optical stereo microscopy

WHY CHOOSE THE TM4000 SERIES

The benchtop SEM from Hitachi makes advanced electron microscopy quick and easy for any user. High resolution, high contrast, large depth-of-focus imaging, and rapid identification of chemical element distribution are achieved with minimal sample preparation time.

Key Capabilities

Quickly optimize your results

With probe current control and voltage control (up to 20kV)

Observe clear topographical contrast

With the dedicated Secondary Electron (SE) detector

Rapidly identify compositional variation

With the Backscatter Electron (BSE) detector

High-resolution imaging

With magnification from 25x to 250,000x

Examine large or multiple specimens

Thanks to the large stage and chamber (samples up to 80mm in diameter and 50mm in height)

Quickly navigate your sample

With the integrated navigation camera and motorized stage*

Get deeper chemical insights

With the x-ray microanalysis (EDX) capability (option), including fast mapping*

Eliminate charging problems on electrically insulating specimens

By switching vacuum mode with a single click

Automate your microscopy and data analysis

With options for multi-field acquisition and automated particle and phase analysis*

Obtain quantitative surface metrology data

Directly in the SEM *

Add advanced detection capabilities

Like STEM or Cathodoluminescence*

Observe dynamic experiments in-situ

With tensile or compression, heating, cooling, electrical probing, and nanoindentation sub-stages*

Features

Flexible Imaging Made Easy

The TM4000 keeps usability and time-to-date at its heart, but this is not at the expense of the flexibility you need to truly understand your sample. Choose between SE (surface contrast) and BSE (compositional contrast) on both conductive and insulating samples without prior sample preparation.

Both SE and BSE detectors can be viewed simultaneously (separately or mixed) as well as in low vacuum mode. The ability to select appropriate probe current and acceleration voltage helps to ensure the best results.

Image: Left: Chemical contrast (BSE) Middle: Topography (SE) Right: Mixed SE/BSE image

Left: Chemical contrast (BSE) Middle: Topography (SE) Right: Mixed SE/BSE image
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Fast Navigation

Thanks to the completely integrated optical navigation camera, users can find their way around their specimen quickly. Users can easily overlay and correlate their SEM and optical images so that they know precisely where they are and what they have done at all times.

Image: The left side shows an SE image of the inside of a watch,  bottom right shows the optical image with overlaid SEM images from areas that have been imaged

High-Performance EDS for Advanced Elemental Analysis

The integrated x-ray microanalysis (EDS) system from leading suppliers like Oxford Instruments or Bruker ensures fast and accurate elemental analysis with advanced features not found on other benchtop SEMs. Live peak deconvolution ensures that spectral line overlaps are removed to provide true elemental distribution and avoid accidental misinterpretation.

Image: Line overlap with W and Si peaks in the spectra on the right By using peak deconvolution it is possible to see which grains actually contain W

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Automate your Particle, Fiber, or Chemical Analysis

Improve your statistics and eliminate time-consuming work by adding our powerful modules to automate your particle, fiber, or matrix analysis (a capability normally associated only with full-size SEMs). Fully automated acquisition and analysis in the TM4000 enables size, morphology, and chemical composition to be quickly characterized, even across thousands or millions of features. This capability can be critical in characterizing materials including:

  • Electrospun fibers
  • Metal powders for additive manufacturing
  • Technical cleanliness (to VDA19 / ISO16232 standards)
  • Steel cleanliness (to ISO4967 standard)
  • Asbestos analysis (to VDI 3492 / ISO14966 standards)
  • Mineral phase identification, liberation, and characterization

Image 1 (left): Left: Automatic particle detection Right: Particle size distribution

Image 2 (bottom left): Mineral particle identification and characterization using Bruker AMICS
Left:BSE image   Middle:Identified particles   Right:Mineral classification

Image 3 (bottom right): Automated fiber thickness measurement

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Examine Wide Areas Automatically

Modules for fully-automated wide-area acquisition and stitching (including imaging and chemical analysis) mean you can get all the high-resolution data you need, even over large length scales.

Image: Geological thin section stitched using 3x3 images to cover a 6x5 mm area

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Quantitative Surface Metrology

Understand your material surfaces in detail with integrated, tilt-free 3D surface modeling and metrology. Measure surface parameters such as depth, angle, or roughness, including 3D surface textures described in ISO 25178.

Image: 3D Surface roughness of a worn metal surface

Cathodoluminescence Detector

The integrated cathodoluminescence detector can detect light emitted from a range of semiconductor, geological and pharmaceutical materials in response to electron beam irradiation. This can be a powerful tool in locating active pharmaceutical ingredients (API) in pharma samples or to undertake geological studies including crystal zonation and growth history.

Image 1:  Sample: Coarse-grained Syenite with zonation in the alkali feldspar
Left: CL image  Middle: BSE image  Right: Mixed CL and BSE

Small variations in Ca and Na content create CL contrast, hardly visible in the BSE image

Image 2: SE, BSE and CL images of a pharmaceutical powder

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Scanning Transmission Electron Microscopy (STEM)

Electron transparent samples such as biological sections or nanoparticles can be imaged with high contrast and surprising ease compared to conventional SEM and TEM. For example, the TM4000 can be used for sample screening prior to full TEM examination, high-throughput imaging of pigments in polymers, or for graphene flake size analysis.

Image: Left: Mouse Kidney Right: Mouse Liver

In-Situ Testing

There are numerous options and accessories to enable in-situ experiments in the TM4000. In situ stages for tilting, rotation, sample manipulation, electrical probing, tensile or compression testing, fatigue testing, nanoindentation, heating, cooling, etc.

Image: Example of tensile testing in the SEM, in this case of a leather sample

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Specifications

Model name TM4000Plus II TM4000 II
Magnifications 10× - 100,000× (Photographic magnification)
25× - 250,000× (monitor display magnification)
Accelerating voltage 5 kV, 10 kV, 15 kV, 20 kV
Image signal Backscattered electron
Secondary electron
Mix (Backscattered electron + Secondary electron)
Backscattered electron
Vacuum mode BSE: Conductor/Standard/Charge-up reduction
SE: Standard/Charge-up reduction
Mix: Standard/Charge-up reduction
BSE: Standard/Charge-up reduction
Sample stage traverse X: 40 mm, Y: 35 mm
Maximum sample size 80 mm (diameter), 50 mm (thickness)
Electron gun Pre-centered cartridge tungsten filament
Signal detection system High-Sensitivity 4-segment BSE detector
High-Sensitivity Low-Vacuum SE detector (UVD)
High-Sensitivity 4-segment BSE detector
Evacuation system
(vacuum pump)
Turbo molecular pump : 67 L/s×1 unit
Diaphragm pump : 20 L/min×1 unit
Size / weight Main unit (motorized stage): 330 (width)×614 (depth)×547 (height) mm, 54 kg
Main unit (manual stage): 330(width)×617(depth)×547(height) mm, 54 kg
Diaphragm pump: 144 (width)×270 (depth)×216 (height) mm, 5.5kg

Speak with our experts

Our service and applications support team can advise on the best product solution for your individual needs.